Identificador persistente para citar o vincular este elemento: http://hdl.handle.net/10553/42779
Título: Microwave assisted micellar extraction coupled with solid phase microextraction for the determination of organochlorine pesticides in soil samples
Autores/as: Vega Moreno, Daura 
Sosa-Ferrera, Zoraida 
Santana Rodríguez, José Juan 
Clasificación UNESCO: 2301 química analítica
Palabras clave: Organochlorine pesticides
Micellar medium
Extraction methods
Microwave
Solid phase microextraction, et al.
Fecha de publicación: 2006
Publicación seriada: Analytica chimica acta (Print) 
Resumen: Microwave assisted micellar extraction (MAME) coupled with solid phase microextraction (SPME) and HPLC-UV determination have been used for the determination of five organochlorine pesticides from agricultural soil samples. A non-ionic surfactant, Polyoxyethlylene 10 Lauryl Ether was used, and the different variables for the optimization of MAME and SPME procedures were studied. This method was applied successfully to the determination of these pesticides in several kinds of agricultural soil samples with different characteristics. Most of the compounds studied can be recovered in good yields with R.S.D. lower than 9% and detection limit ranged between 56–96 ng g−1 for the pesticides studied.
URI: http://hdl.handle.net/10553/42779
ISSN: 0003-2670
DOI: 10.1016/j.aca.2006.04.046
Fuente: Analytica Chimica Acta [ISSN 0003-2670], v. 571 (1), p. 51-57
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