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http://hdl.handle.net/10553/75267
| Title: | Supporting dataset on the optimization and validation of a QuEChERS-based method for the determination of 218 pesticide residues in clay loam soil | Authors: | Acosta-Dacal, Andrea Carolina Rial-Berriel, Cristian Díaz-Díaz, Ricardo Bernal Suárez, Mª del Mar Zumbado, Manuel Henríquez-Hernández, Luis Alberto Pérez Luzardo, Octavio Luis |
UNESCO Clasification: | 2302 Bioquímica 3299 otras especialidades medicas (especificar) 310109 Plaguicidas |
Keywords: | Gc–Ms/Ms Lc-Ms/Ms Matrix Effect Method Optimisation Pesticides, et al |
Issue Date: | 2020 | Journal: | Data in Brief | Abstract: | The dataset presented in this article supports “Optimization and validation of a method for the simultaneous environmental monitoring of 218 pesticide residues in clay loam soil” [1]. A method based on QuEChERS (Quick, Easy, Cheap, Effective, Rugged & Safe) for the extraction of pesticide and some metabolites residues was developed. The quantification of the chemicals was performed by a combination of two complementary LC-MS/MS and GC–MS/MS analyses. Detailed optimization data of the QuEChERS extraction method is provided, including (1) salt combination, (2) acidification of the solvent (3) the amount of the selected acid (Formic Acid, FA) and (4) moisturization of the soil samples prior to extraction. In addition, all the validation data are presented, including the matrix effect, which was evaluated for each analyte using the recommended procedure. | URI: | http://hdl.handle.net/10553/75267 | ISSN: | 2352-3409 | DOI: | 10.1016/j.dib.2020.106393 | Source: | Data in Brief [EISSN 2352-3409], v. 33, 106393 |
| Appears in Collections: | Artículos |
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