Please use this identifier to cite or link to this item: http://hdl.handle.net/10553/47141
DC FieldValueLanguage
dc.contributor.authorVega-Morales, T.en_US
dc.contributor.authorSosa-Ferrera, Z.en_US
dc.contributor.authorSantana-Rodríguez, J. J.en_US
dc.contributor.otherZoraida, Sosa-Ferrera-
dc.contributor.otherVega-Morales, Tanausu-
dc.date.accessioned2018-11-23T11:10:14Z-
dc.date.available2018-11-23T11:10:14Z-
dc.date.issued2011en_US
dc.identifier.issn0039-9140en_US
dc.identifier.urihttp://hdl.handle.net/10553/47141-
dc.description.abstractIn this work, we present the development and application of a microwave assisted extraction followed by liquid chromatography–tandem mass spectrometry methodology (MAE-LC–MS/MS) for the determination of various estradiol-mimicking compounds in sewage sludge samples. For the purification of the MAE extracts, we have employed a solid phase extraction (SPE) clean-up procedure, previously optimised. The entire method provides recoveries between 71.7% and 103.1%, with relative standard deviation lower than 11.1% and limits of detection ranging from 0.6 to 3.5 ng g−1. The developed method was applied to samples from three wastewater treatment plants (WWTPs) located in Las Palmas of Gran Canaria (Spain), two of which had a conventional activated sludge treatment (AST), whereas the third treatment plant had an advanced membrane bioreactor treatment (MBR). All of the analytes in the study, including (nonylphenol (NP), octylphenol (OP), and some of their ethoxylated chains APnEOs (n ≤ 7), 17β-estradiol (E2), estriol (E3), 17α-ethynylestradiol (EE) and bisphenol-A (BPA)), were found in almost all samples in concentrations ranging from 0.9 to 710.2 ng g−1.en_US
dc.languageengen_US
dc.publisher0039-9140-
dc.relation.ispartofTalantaen_US
dc.sourceTalanta [ISSN 0039-9140], v. 85, p. 1825-1834en_US
dc.subject2301 química analíticaen_US
dc.subject.otherAlkylphenolen_US
dc.subject.otherSex hormonesen_US
dc.subject.otherBisphenol-Aen_US
dc.subject.otherMicrowave-assisted extractionen_US
dc.subject.otherLiquid chromatographyen_US
dc.subject.otherMass spectrometryen_US
dc.titleDetermination of various estradiol mimicking-compounds in sewage sludge by the combination of microwave-assisted extraction and LC-MS/MSen_US
dc.typeinfo:eu-repo/semantics/Articlees
dc.typeArticlees
dc.identifier.doi10.1016/j.talanta.2011.07.051
dc.identifier.scopus80052152102-
dc.identifier.isi000295393000021-
dcterms.isPartOfTalanta-
dcterms.sourceTalanta[ISSN 0039-9140],v. 85 (4), p. 1825-1834-
dc.contributor.authorscopusid35328438400-
dc.contributor.authorscopusid6602897915-
dc.contributor.authorscopusid56248783900-
dc.description.lastpage1834-
dc.description.firstpage1825-
dc.relation.volume85-
dc.investigacionCienciasen_US
dc.type2Artículoen_US
dc.identifier.wosWOS:000295393000021-
dc.contributor.daisngid5510888-
dc.contributor.daisngid770178-
dc.contributor.daisngid10914640
dc.contributor.daisngid745012-
dc.identifier.investigatorRIDN-1602-2014-
dc.identifier.investigatorRIDNo ID-
dc.identifier.externalWOS:000295393000021-
dc.contributor.wosstandardWOS:Vega-Morales, T
dc.contributor.wosstandardWOS:Sosa-Ferrera, Z
dc.contributor.wosstandardWOS:Santana-Rodriguez, JJ
dc.date.coverdateSeptiembre 2011
dc.identifier.ulpgces
dc.description.sjr1,429
dc.description.jcr3,794
dc.description.sjrqQ1
dc.description.jcrqQ1
dc.description.scieSCIE
item.fulltextSin texto completo-
item.grantfulltextnone-
crisitem.author.deptGIR Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptGIR Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.orcid0000-0003-3003-3607-
crisitem.author.orcid0000-0002-5635-7215-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.fullNameSosa Ferrera, María Zoraida-
crisitem.author.fullNameSantana Rodríguez, José Juan-
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