Please use this identifier to cite or link to this item: http://hdl.handle.net/10553/36030
DC FieldValueLanguage
dc.contributor.authorAufartová, J.en_US
dc.contributor.authorBrabcová, I.en_US
dc.contributor.authorTorres-Padron, M. E.en_US
dc.contributor.authorSolich, P.en_US
dc.contributor.authorSosa-Ferrera, Z.en_US
dc.contributor.authorSantana-Rodríguez, José Juanen_US
dc.contributor.otherTorres-Padron, Maria Esther-
dc.contributor.otherSolich, Petr-
dc.date.accessioned2018-05-10T08:58:42Z-
dc.date.available2018-05-10T08:58:42Z-
dc.date.issued2017en_US
dc.identifier.issn0889-1575en_US
dc.identifier.urihttp://hdl.handle.net/10553/36030-
dc.description.abstractA new analytical methodology based on ultra-high performance liquid chromatography with fluorescence detection (UHPLC-FD) has been developed for the determination of five fluoroquinolone antibiotics (FQs) used in aquaculture (norfloxacin, ciprofloxacin, enrofloxacin, danofloxacin and sarafloxacin) in fish muscles (e.g. gilthead seabream (Sparus aurata)). The extraction and determination process was carried out by combining microwave-assisted extraction (MAE) along with a clean-up and pre-concentration step with solid phase extraction (SPE) followed by UHPLC-FD detection. The effects of different variables on MAE-SPE were studied and optimized using an experimental design. Validation was made in accordance with Decision 2002/657/EC. CC alpha and CC beta were determined according to the maximum residue limit (MRL). The method detection limit (MDL) of the entire process ranged between 0.1 and 6.0 ng g(-1). The recoveries obtained at two spiked concentrations levels (25 and 250 ng g(-1)) were greater than 90%, and the relative standard deviation was less than 8.7%. The developed methodology was successfully applied for the evaluation of the presence of FQs in fish muscle samples from aquaculture farms bought in various commercial shops in Gran Canaria Island (Spain).en_US
dc.languageengen_US
dc.relation.ispartofJournal of Food Composition and Analysisen_US
dc.sourceJournal Of Food Composition And Analysis [ISSN 0889-1575], v. 56, p. 140-146en_US
dc.subject251002 Oceanografía químicaen_US
dc.subject251092 Acuicultura marinaen_US
dc.subject.otherFood analysisen_US
dc.subject.otherFood compositionen_US
dc.subject.otherMicrowave-assisted extractionen_US
dc.subject.otherFluoroquinolonesen_US
dc.subject.otherSolid-phase extractionen_US
dc.subject.otherUltra-high performance liquiden_US
dc.subject.otherUHPLCen_US
dc.subject.otherMAEen_US
dc.subject.otherSPEen_US
dc.subject.otherGilthead seabreamen_US
dc.subject.otherFishesen_US
dc.subject.otherChromatographyen_US
dc.titleDetermination of fluoroquinolones in fishes using microwave-assisted extraction combined with ultra-high performance liquid chromatography and fluorescence detectionen_US
dc.typeinfo:eu-repo/semantics/Articleen_US
dc.typeArticleen_US
dc.identifier.doi10.1016/j.jfca.2016.12.012
dc.identifier.scopus85006380190-
dc.identifier.isi000393526600018-
dcterms.isPartOfJournal Of Food Composition And Analysis-
dcterms.sourceJournal Of Food Composition And Analysis[ISSN 0889-1575],v. 56, p. 140-146-
dc.contributor.authorscopusid36187944300
dc.contributor.authorscopusid54416951000
dc.contributor.authorscopusid8452532700
dc.contributor.authorscopusid7003997787
dc.contributor.authorscopusid6602897915
dc.contributor.authorscopusid56248783900
dc.identifier.eissn1096-0481-
dc.description.lastpage146-
dc.description.firstpage140-
dc.relation.volume56-
dc.investigacionCienciasen_US
dc.type2Artículoen_US
dc.contributor.daisngid3089112-
dc.contributor.daisngid4269392-
dc.contributor.daisngid22437017
dc.contributor.daisngid2812385-
dc.contributor.daisngid88909-
dc.contributor.daisngid770178-
dc.contributor.daisngid745012-
dc.contributor.daisngid10914640
dc.identifier.investigatorRIDE-9038-2012-
dc.identifier.investigatorRIDB-1851-2009-
dc.utils.revisionen_US
dc.contributor.wosstandardWOS:Aufartova, J
dc.contributor.wosstandardWOS:Brabcova, I
dc.contributor.wosstandardWOS:Torres-Padron, ME
dc.contributor.wosstandardWOS:Solich, P
dc.contributor.wosstandardWOS:Sosa-Ferrera, Z
dc.contributor.wosstandardWOS:Santana-Rodriguez, JJ
dc.date.coverdateMarzo 2017
item.grantfulltextnone-
item.fulltextSin texto completo-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptAnálisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptAnálisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptAnálisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.orcid0000-0001-7000-4419-
crisitem.author.orcid0000-0003-3003-3607-
crisitem.author.orcid0000-0002-5635-7215-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.fullNameTorres Padrón, María Esther-
crisitem.author.fullNameSosa Ferrera, María Zoraida-
crisitem.author.fullNameSantana Rodríguez, José Juan-
crisitem.author.departamentoQuímica-
crisitem.author.departamentoQuímica-
crisitem.author.departamentoQuímica-
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