Please use this identifier to cite or link to this item: http://hdl.handle.net/10553/113970
DC FieldValueLanguage
dc.contributor.authorSantana Viera, Sergio-
dc.contributor.authorCanino Byreing, Alejandro-
dc.contributor.authorTorres Padrón, María Esther-
dc.contributor.authorSosa Ferrera, María Zoraida-
dc.contributor.authorSantana Rodríguez, José Juan-
dc.contributor.authorKabir, Abuzar-
dc.contributor.authorFurton, Kenneth G.-
dc.date.accessioned2022-03-08T13:43:07Z-
dc.date.available2022-03-08T13:43:07Z-
dc.date.issued2022-
dc.identifier.issn2297-8739-
dc.identifier.otherScopus-
dc.identifier.urihttp://hdl.handle.net/10553/113970-
dc.description.abstractAnthracyclines are a group of antineoplastic compounds used to treat acute leukemia and other cancers, and they are excreted after consumption by patients. These chemicals are often found in sewage at very low concentration levels. For this reason, the development of sensitive analytical methodologies capable of determining them at low concentrations is of prime importance. A simple, fast and sensitive analytical method using fabric phase sorptive extraction (FPSE) followed by ultra-high performance liquid chromatography with fluorescence detection (UHPLC-FD) has been developed and validated for the extraction of anthracyclines from sewage samples. FPSE is a green, cheap, simple, selective and rapid sample preparation technique. The different parameters that affect the performance of the FPSE process, including extraction time, eluting solvent, elution time and pH, were optimized. The developed method showed satisfactory reproducibility, with intraday and interday RSD values lower than 15% for all the compounds and limits of detection between 0.1–0.15 µg·L−1. The unique combination of sample preparation by this micro-extraction technique with fluorescence detector have resulted in the satisfactory extraction of highly polar anthracyclines, without any noticeable matrix effect, a very common shortcoming of exhaustive sample preparation technique such as solid phase extraction (SPE) and mass spectrometry.-
dc.languageeng-
dc.relation.ispartofSeparations-
dc.sourceSeparations [EISSN 2297-8739], v. 9 (3), 69, (Marzo 2022)-
dc.subject330201 Tecnología de los antibióticos-
dc.subject330810 Tecnología de aguas residuales-
dc.subject332817 Extracción liquido-liquido-
dc.subject.otherAntineoplastic compounds-
dc.subject.otherEmerging pollutants-
dc.subject.otherFabric phase sorptive extraction-
dc.subject.otherMicroextraction techniques-
dc.subject.otherUltra-high performance liquid cromatography-fluorescense detector-
dc.titleFabric Phase Sorptive Extraction for the Determination of Anthracyclines in Sewage-
dc.typeinfo:eu-repo/semantics/article-
dc.typeArticle-
dc.identifier.doi10.3390/separations9030069-
dc.identifier.scopus85126654662-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.orcidNO DATA-
dc.contributor.authorscopusid56971376800-
dc.contributor.authorscopusid57538067400-
dc.contributor.authorscopusid8452532700-
dc.contributor.authorscopusid6602897915-
dc.contributor.authorscopusid56248783900-
dc.contributor.authorscopusid7005744830-
dc.contributor.authorscopusid7004543580-
dc.identifier.eissn2297-8739-
dc.identifier.issue3-
dc.relation.volume9-
dc.investigacionCiencias-
dc.type2Artículo-
dc.description.notasThis article belongs to the Special Issue High-throughput Analytical Approaches for the Determination of Organic Contaminants in Environmental Samples-
dc.utils.revision-
dc.date.coverdateMarzo 2022-
dc.identifier.ulpgc-
dc.contributor.buulpgcBU-BAS-
dc.description.sjr0,485-
dc.description.jcr2,777-
dc.description.sjrqQ2-
dc.description.jcrqQ3-
dc.description.esciESCI-
dc.description.miaricds8,3-
item.grantfulltextopen-
item.fulltextCon texto completo-
crisitem.author.deptGIR Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptGIR Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptGIR Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.orcid0000-0002-2412-0037-
crisitem.author.orcid0000-0001-7000-4419-
crisitem.author.orcid0000-0003-3003-3607-
crisitem.author.orcid0000-0002-5635-7215-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.fullNameSantana Viera, Sergio-
crisitem.author.fullNameTorres Padrón, María Esther-
crisitem.author.fullNameSosa Ferrera, María Zoraida-
crisitem.author.fullNameSantana Rodríguez, José Juan-
Appears in Collections:Artículos
Thumbnail
Adobe PDF (8,18 MB)
Show simple item record

Google ScholarTM

Check

Altmetric


Share



Export metadata



Items in accedaCRIS are protected by copyright, with all rights reserved, unless otherwise indicated.