Please use this identifier to cite or link to this item: http://hdl.handle.net/10553/53182
DC FieldValueLanguage
dc.contributor.authorMahugo Santana,Cristina Isabelen_US
dc.contributor.authorTorres Padron, M. E.en_US
dc.contributor.authorSosa Ferrera, Z.en_US
dc.contributor.authorSantana Rodríguez, José Juanen_US
dc.contributor.otherZoraida, Sosa-Ferrera-
dc.contributor.otherTorres-Padron, Maria Esther-
dc.date.accessioned2019-02-04T15:30:24Z-
dc.date.available2019-02-04T15:30:24Z-
dc.date.issued2007en_US
dc.identifier.issn0021-9673en_US
dc.identifier.urihttp://hdl.handle.net/10553/47157-
dc.description.abstractA novel analytical method is presented for the determination of chlorophenols in water. This method involves pre-concentration by solid-phase microextraction (SPME) and an external desorption using a micellar medium as desorbing agent. Final analysis of the selected chlorophenols compounds was carried out by high-performance liquid chromatography (HPLC) with diode array detection (DAD). Optimum conditions for desorption, using the non-ionic surfactant polyoxyethylene 10 lauryl ether (POLE), such as surfactant concentration and time were studied. A satisfactory reproducibility for the extraction of target compounds, between 6 and 15%, was obtained, and detection limits were in the range of 1.1–5.9 ng mL−1. The developed method is evaluated and compared with the conventional one using organic solvent as a desorbing agent. The method was successfully applied to the determination of chlorophenols in water samples from different origin. This study has demonstrated that solid-phase microextraction with micellar desorption (SPME-MD) can be used as an alternative to conventional SPME method for the extraction of chlorophenols in water samples.en_US
dc.languageengen_US
dc.publisher0021-9673-
dc.relationAcoplamiento de la Microextracción en Fase Sólida y la Cromatografía Líquida de Alta Resolución Con la Utilización de Medios Micelares Como Extractantes: Desarrollo de Nuevos Métodos Analíticosen_US
dc.relation.ispartofJournal of Chromatography Aen_US
dc.sourceJournal Of Chromatography A [ISSN 0021-9673], v. 1140 (1-2), p. 13-20en_US
dc.subject2301 química analíticaen_US
dc.subject2391 Química ambientalen_US
dc.subject.otherSolid-phase microextractionen_US
dc.subject.otherMicellesen_US
dc.subject.otherChlorophenolsen_US
dc.subject.otherHigh-performance liquid chromatographyen_US
dc.subject.otherWater analysisen_US
dc.titleDevelopment of a solid-phase microextraction method with micellar desorption for the determination of chlorophenols in water samples - Comparison with conventional solid-phase microextraction methoden_US
dc.typeinfo:eu-repo/semantics/Articleen_US
dc.typeArticleen_US
dc.identifier.doi10.1016/j.chroma.2006.11.050en_US
dc.identifier.scopus33845956302-
dc.identifier.isi000243953300002-
dcterms.isPartOfJournal Of Chromatography A-
dcterms.sourceJournal Of Chromatography A[ISSN 0021-9673],v. 1140 (1-2), p. 13-20-
dc.contributor.authorscopusid7006604399-
dc.contributor.authorscopusid8452532700-
dc.contributor.authorscopusid6602897915-
dc.contributor.authorscopusid56248783900-
dc.description.lastpage20en_US
dc.identifier.issue1-2-
dc.description.firstpage13en_US
dc.relation.volume1140en_US
dc.investigacionCienciasen_US
dc.type2Artículoen_US
dc.identifier.wosWOS:000243953300002-
dc.contributor.daisngid2663089-
dc.contributor.daisngid3888969-
dc.contributor.daisngid22437017-
dc.contributor.daisngid770178-
dc.contributor.daisngid1022381-
dc.contributor.daisngid13402121-
dc.contributor.daisngid8799820-
dc.identifier.investigatorRIDN-1602-2014-
dc.identifier.investigatorRIDE-9038-2012-
dc.identifier.externalWOS:000243953300002-
dc.contributor.wosstandardWOS:Santana, CM-
dc.contributor.wosstandardWOS:Padron, MET-
dc.contributor.wosstandardWOS:Ferrera, ZS-
dc.contributor.wosstandardWOS:Rodriguez, JJS-
dc.date.coverdateEnero 2007en_US
dc.identifier.ulpgces
dc.description.jcr3,641
dc.description.jcrqQ1
dc.description.scieSCIE
item.fulltextSin texto completo-
item.grantfulltextnone-
crisitem.project.principalinvestigatorSosa Ferrera, María Zoraida-
crisitem.author.deptGIR IUNAT: Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptGIR IUNAT: Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptGIR IUNAT: Análisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.orcid0000-0001-7000-4419-
crisitem.author.orcid0000-0003-3003-3607-
crisitem.author.orcid0000-0002-5635-7215-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.fullNameMahugo Santana,Cristina Isabel-
crisitem.author.fullNameTorres Padrón, María Esther-
crisitem.author.fullNameSosa Ferrera, María Zoraida-
crisitem.author.fullNameSantana Rodríguez, José Juan-
Appears in Collections:Artículos
Show simple item record

SCOPUSTM   
Citations

47
checked on Jan 22, 2023

WEB OF SCIENCETM
Citations

59
checked on Oct 2, 2022

Page view(s)

29
checked on Dec 3, 2022

Google ScholarTM

Check

Altmetric


Share



Export metadata



Items in accedaCRIS are protected by copyright, with all rights reserved, unless otherwise indicated.