Please use this identifier to cite or link to this item: http://hdl.handle.net/10553/47163
DC FieldValueLanguage
dc.contributor.authorPadrón-Sanz, C.en_US
dc.contributor.authorHalko, R.en_US
dc.contributor.authorSosa-Ferrera, Z.en_US
dc.contributor.authorSantana-Rodríguez, J. J.en_US
dc.contributor.otherZoraida, Sosa-Ferrera-
dc.date.accessioned2018-11-23T11:20:26Z-
dc.date.available2018-11-23T11:20:26Z-
dc.date.issued2005en_US
dc.identifier.issn0021-9673en_US
dc.identifier.urihttp://hdl.handle.net/10553/47163-
dc.description.abstractA new methodology based on the microwave assisted micellar extraction (MAME) technique has been optimised, using soil samples, to extract and determine a mixture of the eight organophosphorous pesticides mainly used in agriculture. The pesticides under study have been extracted using the non-ionic surfactants polyoxyethylene 10 lauryl ether (POLE) and oligoethylene glycol monoalkyl ether (Genapol X-080). The optimal extraction variables, such as surfactant concentration, pH, radiation time and microwave power were determined for each surfactant. The results show the advantage of using POLE instead of Genapol X-080 for the extraction of the organophosphorus pesticides with recoveries higher than 70% for most of the compounds and relative standard deviations (RSD) below 2.6%. This method was successfully applied to fresh samples as well as to aged samples for the analysis of soils with different characteristics and compared with the traditional Soxhlet technique.en_US
dc.languageengen_US
dc.publisher0021-9673-
dc.relation.ispartofJournal of Chromatography Aen_US
dc.sourceJournal of Chromatography A [ISSN 0021-9673], v. 1078, p. 13-21en_US
dc.subject2391 Química ambientalen_US
dc.subject2301 química analíticaen_US
dc.subject.otherOrganophosphorous pesticidesen_US
dc.subject.otherSurfactantsen_US
dc.subject.otherMicrowave assisted micellar extractionen_US
dc.subject.otherHPLC–UVen_US
dc.titleCombination of microwave assisted micellar extraction and liquid chromatography for the determination of organophosphorous pesticides in soil samplesen_US
dc.typeinfo:eu-repo/semantics/Articlees
dc.typeArticlees
dc.identifier.doi10.1016/j.chroma.2005.05.005
dc.identifier.scopus20444476752-
dc.identifier.isi000229996100003-
dcterms.isPartOfJournal Of Chromatography A-
dcterms.sourceJournal Of Chromatography A[ISSN 0021-9673],v. 1078 (1-2), p. 13-21-
dc.contributor.authorscopusid6508056917-
dc.contributor.authorscopusid6603416392-
dc.contributor.authorscopusid6602897915-
dc.contributor.authorscopusid56248783900-
dc.description.lastpage21-
dc.description.firstpage13-
dc.relation.volume1078-
dc.investigacionCienciasen_US
dc.type2Artículoen_US
dc.identifier.wosWOS:000229996100003-
dc.contributor.daisngid7326534
dc.contributor.daisngid5797290-
dc.contributor.daisngid1280756-
dc.contributor.daisngid770178-
dc.contributor.daisngid10914640
dc.contributor.daisngid745012-
dc.identifier.investigatorRIDN-1602-2014-
dc.identifier.externalWOS:000229996100003-
dc.contributor.wosstandardWOS:Padron-Sanz, C
dc.contributor.wosstandardWOS:Halko, R
dc.contributor.wosstandardWOS:Sosa-Ferrera, Z
dc.contributor.wosstandardWOS:Santana-Rodriguez, JJ
dc.date.coverdateJunio 2005
dc.identifier.ulpgces
dc.description.jcr3,096
dc.description.jcrqQ1
item.fulltextSin texto completo-
item.grantfulltextnone-
crisitem.author.deptAnálisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.deptAnálisis Químico Medioambiental-
crisitem.author.deptIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.deptDepartamento de Química-
crisitem.author.orcid0000-0003-3003-3607-
crisitem.author.orcid0000-0002-5635-7215-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.parentorgIU de Estudios Ambientales y Recursos Naturales-
crisitem.author.fullNameSosa Ferrera, María Zoraida-
crisitem.author.fullNameSantana Rodríguez, José Juan-
Appears in Collections:Artículos
Show simple item record

SCOPUSTM   
Citations

69
checked on Jun 20, 2021

WEB OF SCIENCETM
Citations

53
checked on May 2, 2021

Page view(s)

46
checked on Jun 19, 2021

Google ScholarTM

Check

Altmetric


Share



Export metadata



Items in accedaCRIS are protected by copyright, with all rights reserved, unless otherwise indicated.